Applied Online Bubble Size Distribution Measurement in a Pilot Flotation Cell Based on Image Analysis
DOI:
https://doi.org/10.14738/aivp.112.14527Keywords:
Flotation, Image Analysis, BubblesAbstract
The distribution of bubble size in the pulp is a parameter directly related to the flotation kinetics, but its measurement is complex to determine due to the presence of particles and cluster of bubbles. The existing equipment for the measurement of bubble size (McGill and UCT), which operate manually and batch, requires specialized operators in image analysis. On the other hand, the McGill technique has not been directly validated with bubble swarms and only 10% of the sampled bubbles are analyzed. These aspects have limited the technology transfer and sustainability in the measurement of bubble size. To solve the problems presented, a device based on the McGill technique was designed and implemented. Furthermore, algorithms were implemented to increase the statistical significance of the measurement of bubbles per image. The validation consisted of a comparison of the degree of detection using the software manually and automatically (undetected remaining bubbles). As a result, it is possible to predict the bubble size distributions with an error of less than 5% and derivations close to 0.1 [mm] in the determination of D32, using an average of 100 images. In conclusion, the new device and algorithms improve the accuracy of BSD measurements, helping to optimize the process, predict, control flotation kinetics, and be used as a troubleshooting tool. The new device and algorithms improve the accuracy of BSD measurements, helping to optimize the process, predict, control flotation kinetics, and be used as a troubleshooting tool.
References
Rao, S.R., 2003. “Surface Chemistry of Froth Flotation.” Kluwer Academic/Plenum Publishers; 2nd Rev Edition
Loveday, B.K., Brouckaert, C.J.,1995. “An analysis of flotation circuit design principles.” The Chemical Engineering Journal, 59: 15-21.
Nesset, Jan E., Hernandez-Aguilar, J.R., Acuña. C.A., Gomez, C.O., Finch J.A., 2005. “Some gas dispersion characteristics of mechanical flotation machines.” Published by Department of Mining, Metals and Materials Engineering, McGill University, Canada.
Finch, J.A. y Dobby, G.S., 1990. Column Flotation, Pergamon Press: Elmsford, New York, pp. 23-24
Gómez, C.O, Acuna C.A., Girgin E.H., Finch J.A., 2006. “Bubble distributions in laboratory flotation machines measurement and evolution with increasing gas velocity”. International Mineral Processing Congress.
Gómez, C.O., Finch, J.A., 2002. Gas dispersion measurements in flotation machines. CIM Bulletin, Vol. 95 (1066), pp. 73-78.
Grau, R.A., Heiskanen, K., 2003. Gas dispersion measurements in a flotation cell. Minerals Engineering, Vol. 16, pp.1081-1089.
Hernandez-Aguilar, J. R.; Coleman, R. G.; Gomez, C. O. and Finch, J. A. 2004. A comparison between capillary and imaging techniques for sizing bubbles in flotation systems. Minerals Engineering. Volume 17, Issue 1, Pages 53-61. https://doi.org/10.1016/j.mineng.2003.09.011.
X. Bu, S. Zhou, M. Sun, M. Alheshibri, M. S. Khan, G. Xie, et al., Exploring the relationships between gas dispersion parameters and differential pressure fluctuations in a column flotation, ACS Omega 2021 Vol. 6 Issue 34 Pages 21900-21908
Letzel, H. M.; Schouten, J. C.; Krishna, R.; van den Bleek, C. M. Characterization of Regime and Regime Transitions in Bubble Columns by Chaos Analysis of Pressure Signals. Chem. Eng. Sci. 1997, 52, 4447−4459.
Kwon, H. W.; Han, J. H.; Kang, Y.; Sang, D. K. Bubble properties and pressure fluctuations in bubble columns. Korean J. Chem. Eng. 1994, 11, 204−210.
Boyd and Varley, 1998 J.W.R. Boyd and J. Varley, Sound measurement as a means of gas-bubble sizing in aerated agitated tanks, A.I.Ch.E. Journal 44, 1731–1739.
Deen, N. G., Hjertager, B. H., Solberg, T., 2000. Comparison of PIV and LDA measurement methods applied to gas-liquid flow in a bubble column, 10th Int. Symp. on Appl. of Laser Techniques to Fluid Mech., Lisbon, Portugal.
Mondaca, S.; Leiva, C.; Acuña, C. and Serey, E. 2020. “Flow Enhancement of Mineral Pastes to Increase Water Recovery in Tailings: A Matlab-based imaging processing”, Scientific Programming, vol. 2020, 9 pages, 2020. https://doi.org/10.1155/2020/5607242.
Molina, M.; Acuña, C. and Leiva, C. 2020. “Characterization of filamentous flocs to predict sedimentation parameters using image analysis”, Journal of Sensors, febrero 2020, https://doi.org/10.1155/2020/5248509.
Jameson, G.J., Allum, P., 1984. “A survey of bubble sizes in industrial flotation cells.” Reporte a AMIRA'Ltd (Australian Mineral Industries Research Association Limited.
Tucker, J P. Deglon, D A. Franzidis, J -P. Harris, M C., y O'Connor, C T., 1994. “Evaluation of a direct method of bubble size distribution measurement in a laboratory batch flotation cell.” Minerals Engineering, 7: 667-680.
Chen, F., Gomez, C.O., and Finch, J.A., 2001 “Technical note: bubble size measurement in flotation machines.” Minerals Engineering, 14: 427-432.
De Lasa, H., Lee, S.L.P., Bergougnou, M.A., 1984 “Bubble measurement in three-phase fluidized beds using a U-shaped optical fiber.” Canadian Journal of Chemical Engineering, 62: 165-169.
Cathignol, D., Chapelon, J.Y., Newhouse, V.L., Shankar, M., 1988. “Bubble sizing with a high spatial resolution.” Ultrason. Symp. Proc., 2: 933-936.
Grau, R.A., Heiskanen, K., 2002. “Visual technique for measuring bubble size in flotation machines.” Minerals Engineering, 15: 507-513.
Hernandez-Aguilar, J.R., Gomez, C.O., Finch, J.A., 2002. “A technique for the direct measurement of bubble size distributions in industrial flotation cells.” Proc. of the 34th Annual Meeting of the Canadian Mineral Processors, ed. J.E. Nesset: 389-402.
Meernik, P.R., Yuen, M.C., 1988a “Optical method for determining bubble size distributions - Part I. Theory.” Journal of Fluids Engineering-Transactions of the ASME, 110: 325-331.
Meernik, P.R., Yuen, M.C., 1988b. “Optical method for determining bubble size distributions - Part II. Application to bubble size measurement in a three-phase fluidized bed.” Journal of Fluids Engineering-Transactions of the ASME, 110: 332-338.
Randall, E.W., Goodall, C.M., Fairlamb, P.M., Dold, P.L., O’Connor, C.T., 1989. “A method for measuring the sizes of bubbles in two- and three-phase systems.” Journal of Physics E: Scientific Instruments, 22, 827-833.
Acuña, C. and Leiva, C. (2020) Sensor device and system for in-line measurement of bubble-size distribution in flotation cells PCT WO2020132768: World Intellectual Property Organization
Hernandez-Aguilar, J.R., Finch, J.A., 2005. “Validation of bubble sizes obtained with incoherent imaging on a sloped viewing window.” Chemical Engineering Science 60, pp. 14
Acuña, C. A.; and Finch, J. A. 2010. Tracking velocity of multiple bubbles in a swarm. International Journal of Mineral Processing, 94(3-4), 147–158. https://doi:10.1016/j.minpro.2010.02.001.
Redlinger-Pohn, J.; Grabner, M.; Zauner, P.; Radl, S. 2016. Separation of cellulose fibres from pulp suspension by froth flotation fractionation. Separation and Purification Technology, volume 169, pages 304-313. https://doi.org/10.1016/j.seppur.2016.06.004
Schäfer, J.; Schmitt, P.; Hlawitschka, M.; Bart, H. 2019. Measuring Particle Size Distributions in Multiphase Flows Using a Convolutional Neural Network. Chemie Ingenieur Technik, volume 19, Issue 11, pages 1688-1695. https://doi.org/10.1002/cite.201900099
Jamshidi, N.; Mostoufi, N. Investigating bubble dynamics in a bubble column containing shear thinning liquid using a dual-tip probe, Experimental Thermal and Fluid Science, Volume 94, 2018, Pages 34-48. https://doi.org/10.1016/j.expthermflusci.2018.01.034.
Leiva, C., Acuña, C. and Castillo, D. Development and Validation of an Online Analyzer for Particle Size Distribution in Conveyor Belts. Minerals, mayo 2021.
Besagni, G., Brazzale, P., Fiocca, A. and Inzoli, F. Estimation of bubble size distributions and shapes in twophase bubble column using image analysis and optical probes. Flow Measurement and Instrumentation. December 2016.
Mesa, D., Quintanilla, P., and Reyes, F. Bubble Analyser—An open-source software for bubble size measurement using image analysis. Minerals Engineering, April 2022.
Schneider, C. A., Rasband, W. S., and Eliceiri, K. W. NIH Image to Image J: 25 years of image analysis. Nature methods, june 2012.
Tunwal, M., Mulchrone, K. F., and Meere, P. A. Image based particle shape analysis toolbox (IPSAT). Computers & Geosciences, February 2020.
Heilbronner, R. and Barrett, S. Image analysis in earth sciences: Microstructures and textures of earth materials (Vol. 129). Springer Science & Business Media. 2014.
Leiva, C. and Acuña, C. 2021, Dispositivo sensor y sistema para la medición en línea de la distribución del tamaño de burbujas en celdas de flotación, Chile Granted Patent, CL2018003886.
Downloads
Published
How to Cite
Issue
Section
License
Copyright (c) 2023 C.A. Leiva, José Borjas, Claudio Acuña, Saija Luukkanen

This work is licensed under a Creative Commons Attribution 4.0 International License.